Towards the formulation of stable micro and nano double emulsions through silica coating of internal water droplets.

Fiche publication


Date publication

janvier 2019

Journal

Langmuir : the ACS journal of surfaces and colloids

Auteurs

Membres identifiés du Cancéropôle Est :
Pr MELY Yves, Mme MESSADDEQ Nadia


Tous les auteurs :
Akram S, Wang X, Vandamme TF, Collot M, Rehman AU, Messaddeq N, Mély Y, Anton N

Résumé

Delivery systems able to co-encapsulate both hydrophilic and hydrophobic species are of great interest for both fundamental research and industrial applications. Water-in-oil-in-water (w/O/W) emulsions are interesting systems for this purpose, but they suffer from limited stability. In this study we propose an innovative approach to stabilize double emulsions by the synthesis of a silica membrane at the water / oil interface of the primary emulsion ( i.e. inner w/O emulsion). This approach allows the formulation of stable double emulsions through a two-step process, enabling high encapsulation efficiencies of model hydrophilic dyes encapsulated in the internal droplets. This approach also decreases the scale of the double droplets up to the nano-scale, which is not possible without silica stabilization. Different formulation and process parameters were explored in order to optimize the methodology. Physicochemical characterization was performed by dynamic light scattering, encapsulation efficiency measurements, release profiles, as well as by optical and transmission electron microscopies.

Référence

Langmuir. 2019 Jan 10;: