A simple cladding process to apply monolithic silica rods in high performance liquid chromatography.

Fiche publication


Date publication

novembre 2010

Auteurs

Membres identifiés du Cancéropôle Est :
Dr BOOS Anne


Tous les auteurs :
Chamieh J, Zimmermann Y, Boos A, Hagege A

Résumé

A simple cladding procedure was developed to apply monolithic silica rods in chromatography This was used to evaluate the performances of new monolithic silica phases synthesised using a triblock copolymer as a phase separation inducer The cladding procedure is found efficient after several tests including scanning electron microscopy and mercury porosimetry and the obtained columns present a relatively good efficiency in adsorption chromatography (H min is about 50 mu m) as compared to other lab-scale developed columns (C) 2010 Elsevier BV All rights reserved

Référence

J Chromatogr A. 2010 Nov 5;1217(45):7172-6